HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromocyclopentane → 2-(Cyclopentylsulfanyl)pyridine-3-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromocyclopentane | HCID 8728 | — |
| Reactant | HCID 178524460 | HCID 178524460 | — |
| Product | 2-(Cyclopentylsulfanyl)pyridine-3-carboxylic acid | HCID 16787117 | — |
Reaction Steps
2-Mercapto-nicotinic acid (1.0 g, 6.44 mmol) and bromo-cyclopentane (2 mL, 19.33 mmol) were reacted in the same manner as in Step A of Preparation Example 1 to obtain the title compound, which was used in the next step without a separate purification process.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09447044B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-3a309bac34724c338a028dcc1296b76d |
| Source note | uspto-grants-2016_09 |