HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopentanethiol → 2-Cyclopentylsulfanyl-6-methoxy-nicotinic acid methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopentanethiol | HCID 15510 | — |
| Reactant | Methyl 2-chloro-6-methoxynicotinate | HCID 10584232 | — |
| Product | 2-Cyclopentylsulfanyl-6-methoxy-nicotinic acid methyl ester | HCID 90118163 | 77% |
Reaction Steps
2-Chloro-6-methoxy-nicotinic acid methyl ester (54 mg, 0.26 mmol) and cyclopen-tanethiol were reacted in the same manner as in Step A of Preparation Example 16 to obtain the title compound (55 mg, 77%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09447044B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-e70926e9fcc74d7ca1763b3f81742b6f |
| Source note | uspto-grants-2016_09 |