HRID62902

反应详情

EQUATION

反应方程式

HRID 62902 的结构方程式

PROCEDURE

实验过程

After 2-(4-benzyloxy-3,5-difluoro-phenyl)-cyclopropanecarboxylic acid (75 mg, 0.246 mmol) was dissolved in anhydrous MC (5 ml), SOCl2 (0.58 g, 4.92 mmol) was added thereto, and the mixture was stirred at room temperature for 18 hours. After the termination of the reaction, the reactant was concentrated under reduced pressure to obtain the title compound, which was used in the next step without a separate purification process.

WORKUP

后处理

  1. additionwas added
  2. customAfter the termination of the reaction
  3. concentrationthe reactant was concentrated under reduced pressure