HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 629020Generated: October 31, 2026
Dicyclohexylcarbodiimide → HCID 70975398, compound
https://huagongshe.com/reaction/629020
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | HCID 86673506 | HCID 86673506 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 70975398 | HCID 70975398 | 73% |
Reaction Steps
A suspension of 1-(2-aminophenyl)-3-(4-(5-(methylthio)-4-morpholinopyrimidin-2-yl)phenyl)thiourea (60 mg, 0.132 mmole) and dicyclohexylcarbodiimide (31 mg, 0.15 mmole) in THF (5 ml) was heated at 64° C. for 20 hr. The cooled mixture was purified by flash chromatography to give a product (40 mg, 73%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09315491B2 |
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| Source dataset | uspto-grants-2016_04 |
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| ORD ID | ord-72758a4e155540a6af17871e6547a40d |
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| Source note | uspto-grants-2016_04 |
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