3-Iodobenzoic acid → N-(3-fluoro-4-(trifluoromethoxy)phenyl)-3-iodobenzamide

関与物質

反応手順

The title compound was prepared in an analogous fashion to that described in Stage 30.1 using 3-iodobenzoic acid and 3-fluoro-4-(trifluoromethoxy)aniline to afford the title compound as a white solid. UPLC-MS (Condition 1) tR=3.39 min, m/z=425.9 [M+H]+, m/z=423.9 [M−H]−; 1H-NMR (400 MHz, DMSO-d6) δ ppm 7.32-7.40 (m, 1H) 7.54-7.62 (m, 1H) 7.64 (dd, 1H) 7.93-8.01 (m, 3H) 8.29 (s, 1H) 10.64 (s, 1H).

情報源と証拠