HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-1-benzofuran-2-carbaldehyde → 5-Butyl-2-formylbenzofuran
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-1-benzofuran-2-carbaldehyde | HCID 2795535 | — |
| Reactant | Potassium Butyltrifluoroborate | HCID 23693579 | — |
| Product | 5-Butyl-2-formylbenzofuran | HCID 115493583 | 90% |
Reaction Steps
The compound was synthesized as in Example 3.1, using 5-bromo-2-formylbenzofuran (500 mg, 2.22 mmol) in place of 5-bromo-2-formylfuran and potassium butyltrifluoroborate (546 mg, 3.33 mmol) in place of hexylboronic acid to give 5-butyl-2-formylbenzofuran (402 mg, 90%). Used without further characterization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315495B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-7e2fe99bdb704e07849ab317f546aee4 |
| Source note | uspto-grants-2016_04 |