HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Butyltrifluoroborate → Methyl-6-butylbenzofuran-2-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Butyltrifluoroborate | HCID 23693579 | — |
| Reactant | Methyl 6-bromo-1-benzofuran-2-carboxylate | HCID 59015856 | — |
| Product | Methyl-6-butylbenzofuran-2-carboxylate | HCID 118228973 | 67% |
Reaction Steps
Methyl-6-butylbenzofuran-2-carboxylate was synthesized as in Example 3.1 using methyl-6-bromobenzofuran-2-carboxylate (195 mg, 0.76 mmol) in place of 5-bromo-2-formylfuran and potassium butyltrifluoroborate (188 mg, 1.15 mmol) in place of hexylboronic acid to give methyl-6-butylbenzofuran-2-carboxylate (118 mg, 67%). Used without further characterization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315495B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-63a809f89f9d40b985e6c741c53da17a |
| Source note | uspto-grants-2016_04 |