HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-methylbenzaldehyde → 2-Methyl-4-butylbenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-methylbenzaldehyde | HCID 13555150 | — |
| Reactant | Potassium Butyltrifluoroborate | HCID 23693579 | — |
| Product | 2-Methyl-4-butylbenzaldehyde | HCID 118228974 | 35% |
Reaction Steps
The compound was synthesized as in Example 3.1 using 2-methyl-4-bromobenzaldehyde (113 mg, 0.57 mmol) in place of 5-bromo-2-formylfuran and potassium butyltrifluoroborate (113 mg, 0.69 mmol) in place of hexylboronic acid to give 2-methyl-4-butylbenzaldehyde (34 mg, 35%). Used without further characterization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315495B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-eb46a0acf6184148b18cb68e5587639e |
| Source note | uspto-grants-2016_04 |