HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Bromobenzo[b]thiophene-2-carbaldehyde → HCID 118230501, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Bromobenzo[b]thiophene-2-carbaldehyde | HCID 56832309 | — |
| Reactant | Potassium 3,3,3-trifluoropropane-1-trifluoroborate | HCID 56972906 | — |
| Product | HCID 118230501 | HCID 118230501 | 80% |
Reaction Steps
The compound was synthesized as in Example 3.1 using 6-bromobenzothiophene-2-carbaldehyde (50 mg, 0.21 mmol) in place of 5-bromo-2-formylfuran and potassium (3,3,3-trifluoro)propyltrifluoroborate (63 mg, 0.31 mmol) in place of hexylboronic acid to give 6-(3,3,3-trifluoropropyl)benzothiophene-2-carbaldehyde (43 mg, 80%). Used without further characterization.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315495B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-7c3f69e3c5f44175b15bd924c84fd03d |
| Source note | uspto-grants-2016_04 |