HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 118222818, compound → 1-Methyl-5-propoxy-1H-indole-2-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 118222818 | HCID 118222818 | — |
| Reactant | (1-methyl-5-propoxy-1H-indol-2-yl)methanol | HCID 118222834 | — |
| Product | 1-Methyl-5-propoxy-1H-indole-2-carbaldehyde | HCID 118222786 | 75% |
Reaction Steps
1-Methyl-5-propoxy-1H-indole-2-carbaldehyde (60 mg, 75% over two steps) was synthesized by the same reduction/oxidation sequence as in Example 52.1, using ethyl 1-methyl-5-propoxy-1H-indole-2-carboxylate (96 mg, 0.37 mmol) in place of methyl-6-butylbenzofuran-2-carboxylate, and (1-methyl-5-propoxy-1H-indol-2-yl)methanol (60 mg, 0.27 mmol) in place of (6-butylbenzofuran-2-yl)methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315495B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-f11569499b634fc6857f55b17ba147fe |
| Source note | uspto-grants-2016_04 |