HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → IDF-11774
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | PMID26882240-Compound-8 | HCID 625381 | — |
| Product | IDF-11774 | HCID 71542096 | 93.3% |
Reaction Steps
The title compound was prepared from 2-(4-(adamantan-1-yl)phenoxy)acetic acid (2.0 g, 6.98 mmol) and 1-methylpiperazine (0.69 g, 6.98 mmol) according to the example 1, which was given 2-(4-(adamantan-1-yl)phenoxy)-1-(4-methylpiperazin-1-yl)ethanone as a white solid (2.4 g, 93.3% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315507B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-737ce298dc78430d8ff5c9f49900f754 |
| Source note | uspto-grants-2016_04 |