HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → HCID 71542491, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | HCID 86729439 | HCID 86729439 | — |
| Product | HCID 71542491 | HCID 71542491 | 92.5% |
Reaction Steps
The title compound was prepared from 2-(4-(adamantan-1-yl)-2-chlorophenoxy)acetic acid (0.2 g, 0.62 mmol), prepared from the step 4, and 1-methylpiperazine (0.062 g, 0.62 mmol) according to the example 1, which was given 2-(4-(adamantan-1-yl)-2-chlorophenoxy)-1-(4-methylpiperazin-1-yl)ethanone as a white solid (0.231 g, 92.0% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315507B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-ac4e74c9162443359d5f0bb9efbed7c6 |
| Source note | uspto-grants-2016_04 |