HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphoric Acid → HCID 71542757, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphoric Acid | HCID 1004 | — |
| Reactant | IDF-11774 | HCID 71542096 | — |
| Product | HCID 71542757 | HCID 71542757 | 75.4% |
Reaction Steps
The title compound was prepared from 2-(4-(adamantan-1-yl)phenoxy)-1-(4-methylpiperazin-1-yl)ethanone (1.0 g, 2.7 mmol), prepared from the example 3, and phosphoric acid (0.19 mL, 2.7 mmol) according to the example 43, which was given 4-(2-(4-(adamantan-1-yl)phenoxy)acetyl)-1-methylpiperazin-1-ium dihydrogenphosphate as a crystalline white solid (0.95 g, 75% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315507B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-e5cf4c596acc40058245846399c7f4c3 |
| Source note | uspto-grants-2016_04 |