HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → N-(2,3-Dihydro-5-benzofuranyl)acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | 2,3-Dihydro-1-benzofuran-5-amine | HCID 3841102 | — |
| Solvent | Acetic Anhydride | HCID 7918 | — |
| Product | N-(2,3-Dihydro-5-benzofuranyl)acetamide | HCID 12908576 | 88% |
Reaction Steps
The product (5.2 g, 38.5 mmol) obtained in Step 2 was dissolved in AcOH (20 mL) and Ac2O (5 mL), heated to 60° C., reacted for 12 h, and concentrated to obtain a crude product (6 g, 88.0%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315513B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-d8cd9c2594d146538e09f239e153ba7a |
| Source note | uspto-grants-2016_04 |