HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Nitro-2,3-dihydrobenzofuran-5-amine → HCID 53420116, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Nitro-2,3-dihydrobenzofuran-5-amine | HCID 13069187 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53420116 | HCID 53420116 | — |
Reaction Steps
The product obtained in Step 5 (2.5 g, 13.9 mmol) and Pd/C (0.5 g) were dissolved in EtOH (50 mL), hydrogenated in a Parr hydrogenation apparatus at room temperature and a hydrogen pressure of 50 PSI for 12 h. The catalyst was removed by filtration, the ethanol solution of the product was directly used in the next step of reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315513B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-02a7d3eeb73a4c6fbc41806e5940cffe |
| Source note | uspto-grants-2016_04 |