4-Nitro-1H-indazol-5-amine → HCID 68264363, compound

HRID 629686Notes

Reaction equation

HRID 629686 reaction equation
[N+:1]([C:4]1[C:12]([NH2:13])=[CH:11][CH:10]=[C:9]2[C:5]=1[CH:6]=[N:7][NH:8]2)([O-])=O>[Pd]>[NH2:1][C:4]1[C:12]([NH2:13])=[CH:11][CH:10]=[C:9]2[C:5]=1[CH:6]=[N:7][NH:8]2

Participants

3

Reactant 1

HCID 682646554-Nitro-1H-indazol-5-amine

Product 1

HCID 68264363HCID 68264363, compoundYield 67.5%

Reagents, catalysts & solvents 1

HCID 23938PalladiumCatalyst

Procedure

By referring to the Step 6 of Example 1, 4-nitro-5-aminoindazole (2.5 g, 14.0 mmol), Pd/C (0.25 g), were used to obtain a product (1.4 g, 65.5%).

Sources & evidence

ORD record
ord-8ce135b3ec5f46baaea4b5ff738ff4f5
Source dataset
uspto-grants-2016_04
Patent number
US09315513B2

Reaction notes

Loading…