HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitric Acid → 5,6-Dinitro-1H-indazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitric Acid | HCID 944 | — |
| Reactant | 6-Nitroindazole | HCID 24239 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 5,6-Dinitro-1H-indazole | HCID 96063 | 28.6% |
Reaction Steps
By referring to the Step 1 of Example 7, 6-nitroindazole (5 g, 30.7 mmol), 35 mL of acetic acid, concentrated HNO3 (3.6 mL, 181.6 mmol), were used to obtain a product (1.8 g, 28.6%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315513B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-efd5e04f12e845a8a3674bc03824a8f7 |
| Source note | uspto-grants-2016_04 |