HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 3-(3-fluoro-4-hydroxyphenyl)propionate → HCID 90118258, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 3-(3-fluoro-4-hydroxyphenyl)propionate | HCID 3023769 | — |
| Reactant | 3-Chloromethyl-2-cyclopropylmethylsulfanyl-pyridine | HCID 90118184 | — |
| Product | HCID 90118258 | HCID 90118258 | 87% |
Reaction Steps
3-Chloromethyl-2-cyclopropylmethylsulfanyl-pyridine (0.030 g, 0.14 mmol) obtained in Step C of Preparation Example 18 and 3-(3-fluoro-4-hydroxy-phenyl)-propionic acid ethyl ester (0.031 g, 0.14 mmol) obtained in Step C of Preparation Example 6 were used to react sequentially in the same manner as in Steps A and B of Example 1 to obtain the title compound (0.044 g, 86%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09447044B2 |
| Source dataset | uspto-grants-2016_09 |
| ORD ID | ord-841fb188046e45f88aaed6c71a4790cb |
| Source note | uspto-grants-2016_09 |