HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178483938, compound → HCID 178483937, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178483938 | HCID 178483938 | — |
| Reactant | HCID 178493271 | HCID 178493271 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178483937 | HCID 178483937 | — |
Reaction Steps
Obtained as a light brown oil (94%) starting from trans-4-((3-(2-chloro-4-(hydroxy-methyl)phenylamino)-3-oxopropyl)(methyl)amino)cyclohexyl hydroxy(di-2-thienyl)-acetate (intermediate 49; 0.06 g, 0.11 mmol) and manganese (IV) oxide (0.098 mg, 1.13 mmol) in chloroform (1.4 mL) following the experimental procedure as described for intermediate 43.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09315463B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-561c99c7fc4545728e267b94232a115b |
| Source note | uspto-grants-2016_04 |