Dimethyl Sulfone → HCID 118671891, compound

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Reaction Steps

The target compound was obtained in three chemical steps from 68a). In the first step, compound 68a) was oxidized to the corresponding methylsulfone with use of m-chloroperoxybenzoic acid. The methylsulfone was then reacted with sodium azide and afterwards hydrogenated in analogy to the procedures 68b) and 68c), respectively. White solid. Yield: 75 mg. HPLC-MS (method 4): Rt=2.72 min; m/z [M+H]+=479.9

Provenance & Evidence