Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 630531Generated: November 1, 2026

m-Chloroperbenzoic acid → HCID 118666103, compound

https://huagongshe.com/reaction/630531

Reaction equation

Participants

RoleNameHCIDCharge
Reactantm-Chloroperbenzoic acidHCID 70297—
ReactantO-(Benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborateHCID 2733207—
ReactantD-beta-ProlinolHCID 7446913—
ReactantHCID 118666170HCID 118666170—
ProductHCID 118666103HCID 118666103—

Reaction Steps

Prepared from 1-(5-(2-fluorophenyl)pyrimidin-2-yl)-3-(methylthio)-1H-indole-6-carboxylic acid in two reaction steps comprising a TBTU mediated amide coupling with (R)-pyrrolidin-3-ylmethanol (see also procedure 244c) and an oxidation utilizing m-chloroperoxybenzoic acid as oxidizing agent. Yellow solid. Yield: 0.12 g

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09315490B2
Source datasetuspto-grants-2016_04
ORD IDord-7ecff4b297a045dfa1e62eb956b6681d
Source noteuspto-grants-2016_04