Imidazole → HCID 22229102, compound

Participants

Reaction Steps

1 part by weight of glycidyl ether and 2.5 to 5 parts by weight of acryloyl chloride are added into a three-neck flask, and then 15 to 25 parts by weight of N,N-dimethyl formamide as a solvent, and 0.1 to 0.5 parts by weight of imidazole as a reaction promoter are added therein. The reactants are heated to 90° C. to 140° C. with stirring under N2 atmosphere and the reaction is kept for 4 to 24 h. Then the solvent of N,N-dimethyl formamide is removed by reduced pressure distillation, and the residual is dried under vacuum to obtain the glycidyl ether-acrylate polymerizable monomer.

Provenance & Evidence