化工社化工社 化学情報印刷レポート · 研究参考用
1,2,3-Trichloropropane → 1,1,2,3-Tetrachloro-1-propene
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1,2,3-Trichloropropane | HCID 7285 | — |
| 反応物 | Fenteracol | HCID 16462 | — |
| 反応物 | 1,1,2,2,3-Pentachloropropane | HCID 85562 | — |
| 反応物 | Propane, pentachloro- | HCID 186684 | — |
| 反応物 | 1,1,1,2,3-Pentachloropropane | HCID 13454491 | — |
| 生成物 | 1,1,2,3-Tetrachloro-1-propene | HCID 25281 | — |
| 生成物 | 1-Propene, 2,3,3,3-tetrachloro- | HCID 588742 | — |
反応手順
The overhead stream comprising 1,2,3-trichloropropane, TCPE, tetrachloropropanes, 1,1,2,2,3-pentachloropropane, 1,1,1,2,3-pentachloropropane, and 1,1,1,2,2-pentachloropropane is then provided to a reactor where it is dehydrochlorinated to provide dichloropropenes, trichloropropenes, 2,3,3,3-tetrachloropropene, and 1,1,2,3-tetrachloropropene. More specifically, dehydrochlorination reactor may typically be a batch or a continuous stirred tank reactor. The mixing can be done, e.g., by mechanical or jet mixing of feed streams. Those of ordinary skill in the art are readily able to determine the appropriate conditions at which to run a dehydrochlorination reactor in order to conduct the aforementioned dehydrochlorination.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09321707B2 |
| 出典データセット | uspto-grants-2016_04 |
| ORD ID | ord-3982892dfcc3409083277abf43af557c |
| 出典メモ | uspto-grants-2016_04 |