Methanol → HCID 89825964, compound

Participants

Reaction Conditions

Reaction Steps

Sodium (45 mg, 1.96 mmol) was dissolved in methanol (1.5 ml), N-(6-bromo-4-methyl-2-pyridyl)ethane-1,2-diamine (69 mg, 0.3 mmol) was added and the resulting mixture was stirred under microwave heating at 140° C. for three hours. The mixture was concentrated under reduced pressure and the residue was washed several times with ethyl acetate and acetonitrile. The washing solutions were decanted from the solid, the combined washing solutions were evaporated to dryness under reduced pressure to yield 58 mg. MS(ESI) m/z=182.0 [M+1]+.

Provenance & Evidence