N-Methylethylamine → HCID 71093608, compound

HRID 632330Notes

Reaction equation

HRID 632330 reaction equation
[CH:1]1([C:4]2[CH:5]=[CH:6][C:7]([C:15]([NH:17][C:18]([CH2:24][CH3:25])([CH2:22][CH3:23])[C:19]([OH:21])=O)=[O:16])=[N:8][C:9]=2[O:10][CH2:11][CH:12]2[CH2:14][CH2:13]2)[CH2:3][CH2:2]1.[CH3:26][NH:27][CH2:28][CH3:29]>>[CH2:24]([C:18]([NH:17][C:15]([C:7]1[CH:6]=[CH:5][C:4]([CH:1]2[CH2:2][CH2:3]2)=[C:9]([O:10][CH2:11][CH:12]2[CH2:14][CH2:13]2)[N:8]=1)=[O:16])([C:19](=[O:21])[N:27]([CH2:28][CH3:29])[CH3:26])[CH2:22][CH3:23])[CH3:25]

Participants

3

Reactant 2

HCID 12219N-MethylethylamineHCID 710875422-(5-Cyclopropyl-6-(cyclopropylmethoxy)picolinamido)-2-ethylbutanoic acid

Product 1

HCID 71093608HCID 71093608, compound

Procedure

The title compound was synthesized in analogy to Example 1, using 2-(5-cyclopropyl-6-(cyclopropylmethoxy)picolinamido)-2-ethylbutanoic acid (Example 274 a) and N-methylethanamine (CAN 624-78-2) as starting materials. MS (EI): m/e=388.0 [M+H]+.

Sources & evidence

ORD record
ord-929edd7ef6c341feb1fdb22537e00433
Source dataset
uspto-grants-2016_04
Patent number
US09321727B2

Reaction notes

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