Ethanamine, 2-((trimethylsilyl)oxy)- (9CI) → HCID 71093561, compound
Reaction equation
[CH:1]1([C:4]2[CH:5]=[CH:6][C:7]([C:15]([NH:17][C:18]([CH2:24][CH3:25])([CH2:22][CH3:23])[C:19](O)=[O:20])=[O:16])=[N:8][C:9]=2[O:10][CH2:11][CH:12]2[CH2:14][CH2:13]2)[CH2:3][CH2:2]1.C[Si](C)(C)[O:28][CH2:29][CH2:30][NH2:31]>>[CH2:24]([C:18]([NH:17][C:15]([C:7]1[CH:6]=[CH:5][C:4]([CH:1]2[CH2:2][CH2:3]2)=[C:9]([O:10][CH2:11][CH:12]2[CH2:14][CH2:13]2)[N:8]=1)=[O:16])([C:19](=[O:20])[NH:31][CH2:30][CH2:29][OH:28])[CH2:22][CH3:23])[CH3:25]Participants
3
Procedure
The title compound was synthesized in analogy to Example 1, using 2-(5-cyclopropyl-6-(cyclopropylmethoxy)picolinamido)-2-ethylbutanoic acid (Example 274 a) and 2-(trimethylsilyloxy)ethanamine (CAN 5804-92-2)-as starting materials. MS (EI): m/e=390.5 [M+H]+.
Sources & evidence
- ORD record
- ord-f50556f04ede4630919031f785aaa9c7
- Source dataset
- uspto-grants-2016_04
- Patent number
- US09321727B2
Reaction notes
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