HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl(2-pyridylmethyl)amine → HCID 58614708, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl(2-pyridylmethyl)amine | HCID 88757 | — |
| Reactant | 3-Chloro-4-(4-chloro-3-(pyridin-2-yl)phenylcarbamoyl)benzoic acid | HCID 66878605 | — |
| Product | HCID 58614708 | HCID 58614708 | — |
Reaction Steps
40 mg of 3-chloro-4-(4-chloro-3-(pyridin-2-yl)phenylcarbamoyl)benzoic acid was coupled to N-methyl-1-(pyridin-2-yl)methanamine via Procedure G. The crude product was purified on reverse phase HPLC to yield 2-chloro-N1-(4-chloro-3-(pyridin-2-yl)phenyl)-N4-methyl-N4-(pyridin-2-ylmethyl)terephthalamide. MS (Q1) 491 (M)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09321761B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-6941a2d8a2ff4fbea5931786238fef72 |
| Source note | uspto-grants-2016_04 |