HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-chloro-N-(4-chloro-3-(pyridin-2-yl)phenyl)-2-methylnicotinamide → HCID 178433153, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-chloro-N-(4-chloro-3-(pyridin-2-yl)phenyl)-2-methylnicotinamide | HCID 58614798 | — |
| Reactant | HCID 178419017 | HCID 178419017 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 178433153 | HCID 178433153 | — |
Reaction Steps
Procedure F was performed using 60 mg of 6-chloro-N-(4-chloro-3-(pyridin-2-yl)phenyl)-2-methylnicotinamide and 93 mg of histamine in 0.5 mL of BuOH. Purified by reverse phase HPLC to yield 6-(2-(1H-imidazol-4-yl)ethylamino)-N-(4-chloro-3-(pyridin-2-yl)phenyl)-2-methylnicotinamide. MS (Q1) 433.0 (M)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09321761B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-d6e49be0af99429785742f275acc33eb |
| Source note | uspto-grants-2016_04 |