HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66877087, compound → HCID 178512137, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66877087 | HCID 66877087 | — |
| Reactant | HCID 178510931 | HCID 178510931 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178512137 | HCID 178512137 | — |
Reaction Steps
Ethyl 4-(4-chloro-3-(pyridin-2-yl)phenylcarbamoyl)benzimidate (2.0 ml of a 0.075 M methanol solution, 0.15 mmol) was treated with 3-(1H-imidazol-4-yl)propan-1-amine (27 μl, 0.23 mmol) via procedure W to afford 83 mg of 4-(N-(3-(1H-imidazol-4-yl)propyl)carbamimidoyl)-N-(4-chloro-3-(pyridin-2-yl)phenyl)benzamide. MS (Q1) 459 (M)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09321761B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-59266628b3a147ff8b4018000184092b |
| Source note | uspto-grants-2016_04 |