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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 633335Generated: October 29, 2026

Piperidine → HCID 58614731, compound

https://huagongshe.com/reaction/633335

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPiperidineHCID 8082—
ReactantHCID 66877087HCID 66877087—
ProductHCID 58614731HCID 58614731—

Reaction Steps

Ethyl 4-(4-chloro-3-(pyridin-2-yl)phenylcarbamoyl)benzimidate (17.5 ml of a 0.0155 M solution, 0.27 mmol) was treated with piperidine (1.0 ml, 10.0 mmol) for 3 days. The ethanol was evaporated, and the residue purified by reverse phase HPLC to afford 26 mg of N-(4-chloro-3-(pyridin-2-yl)phenyl)-4-(imino(piperidin-1-yl)methyl)benzamide. MS (Q1) 419 (M)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09321761B2
Source datasetuspto-grants-2016_04
ORD IDord-196f8ee44379496f8ced36fe63d12bee
Source noteuspto-grants-2016_04