HCID 90417101, compound → HCID 90417231, compound

Participants

Reaction Steps

A mixture of Example 2C (0.165 g, 0.401 mmol) and 10% palladium on carbon (0.043 g, 0.040 mmol) in ethyl acetate (10 mL) was treated with a balloon of hydrogen gas. The reaction mixture was stirred for 10 hours at ambient temperature. The solid was removed by filtration, and the filtrate was concentrated to give the title compound (0.152 g, 0.399 mmol, 99% yield).

Provenance & Evidence