HCID 178494054, compound → HCID 178494053, compound

Participants

Reaction Steps

A mixture of Example 6B (0.025 g, 0.061 mmol) in tetrahydrofuran (10 mL) was added to 10% palladium on carbon (0.005 g, 0.047 mmol) in a 50 mL pressure bottle and stirred at ambient temperature under hydrogen at 30 psi for 2 hours. The solid was removed by filtration, and the filtrate was concentrated to provide the title compound (0.023 g, 100% yield).

Provenance & Evidence