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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 633529Generated: October 30, 2026

HCID 90416587, compound → HCID 90417049, compound

https://huagongshe.com/reaction/633529

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 90416587HCID 90416587—
CatalystPalladiumHCID 23938—
SolventTetrahydrofuranHCID 8028—
ProductHCID 90417049HCID 9041704999%

Reaction Steps

A solution of Example 15A (167 mg, 0.425 mmol) in tetrahydrofuran (20 mL) was added to 10% palladium on carbon (34 mg, 0.319 mmol) in a 50 mL pressure bottle and stirred at ambient temperature under hydrogen at 30 psi for 1 hour. The solution was filtered through a syringe filter and concentrated to give the title compound (152 mg, 99%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09321764B2
Source datasetuspto-grants-2016_04
ORD IDord-613fe2c0ec9248a39b8ff7a987f7107e
Source noteuspto-grants-2016_04