HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 90416587, compound → HCID 90417049, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 90416587 | HCID 90416587 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 90417049 | HCID 90417049 | 99% |
Reaction Steps
A solution of Example 15A (167 mg, 0.425 mmol) in tetrahydrofuran (20 mL) was added to 10% palladium on carbon (34 mg, 0.319 mmol) in a 50 mL pressure bottle and stirred at ambient temperature under hydrogen at 30 psi for 1 hour. The solution was filtered through a syringe filter and concentrated to give the title compound (152 mg, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09321764B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-613fe2c0ec9248a39b8ff7a987f7107e |
| Source note | uspto-grants-2016_04 |