N-Iodosuccinimide → HCID 90417079, compound

Participants

Reaction Steps

The product from Example 91B (0.82 g, 3.40 mmol) and N-iodosuccinimide (0.918 g, 4.08 mmol) were combined in dimethylformamide (17.01 mL), stirred for two hours at ambient temperature, and quenched with 100 mL of 10% aqueous sodium thiosulfate. The mixture was stirred for 15 minutes and the resulting solid was collected by filtration, washed repeatedly with water and dried to constant mass to afford the title compound (1.17 g, 94%).

Provenance & Evidence