Ethanol → HCID 90416203, compound

Participants

Reaction Steps

The product from Example 92A (0.04 g, 0.083 mmol) and 10% Pd/C (0.022 g, 0.021 mmol) were combined in ethyl acetate (3 mL)/ethanol (3 mL), degassed under vacuum, placed under a balloon of hydrogen and stirred for 2 hours. The mixture was filtered through Celite and the Celite pad was washed repeatedly with ethyl acetate. The filtrate was concentrated to afford the title compound (0.042 g, 105%).

Provenance & Evidence