Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 634448Generated: October 29, 2026

Potassium Carbonate → HCID 118131024, compound

https://huagongshe.com/reaction/634448

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant1H-Pyrazolo[3,4-d]pyrimidin-4-amineHCID 75420—
ReactantHCID 118131409HCID 118131409—
SolventDimethylformamideHCID 6228—
ProductHCID 118131024HCID 1181310243%

Reaction Steps

The title compound was made in a similar way as that of the compound of example 15, 3-(1-bromoethyl)-4-(2-methylpyridin-4-yl)-1H-isochromen-1-one (intermediate C14, 98 mg, 0.285 mmol), 1H-pyrazolo[3,4-d]pyrimidin-4-amine (57.7 mg, 0.43 mmol) and K2CO3 (59 mg, 0.42 mmol) in DMF (2 ml) at 50° C. for 6 hrs to give the title compound (3.4 mg, 3%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09321776B2
Source datasetuspto-grants-2016_04
ORD IDord-2d3fe5a547814a2c9cb0602e723cc3c3
Source noteuspto-grants-2016_04