HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxy-6-(tributylstannyl)pyrazine → HCID 178438189, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxy-6-(tributylstannyl)pyrazine | HCID 16427103 | — |
| Reactant | 3-(1-(4-Amino-3-iodo-1H-pyrazolo[3,4-d]pyrimidin-1-yl)ethyl)-4-phenyl-1H-isochromen-1-one | HCID 118131053 | — |
| Product | HCID 178438189 | HCID 178438189 | 36.8% |
Reaction Steps
The title compound was made in a similar way as that of the compound of example 89 from 3-(1-(4-amino-3-iodo-1H-pyrazolo[3,4-d]pyrimidin-1-yl)ethyl)-4-phenyl-1H-isochromen-1-one (intermediate D2a, 120 mg, 0.236 mmol) and 2-methoxy-6-(tributylstannyl)pyrazine (188 mg, 0.471 mmol) to give the title compound (25 mg, 36.8%) as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09321776B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-76c44539010a4c5eb52b826d6e1e7936 |
| Source note | uspto-grants-2016_04 |