HuagongsheHuagongshe Chemistry Print Report · For research reference only
Homophenylalanine, DL- → 2-Amino-4-phenylbutan-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Homophenylalanine, DL- | HCID 102530 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Product | 2-Amino-4-phenylbutan-1-ol | HCID 13145036 | 78.1% |
Reaction Steps
Following the general procedure of example 40b, DL-homophenylalanine (5.0 g, 27.9 mmol) was reduced with LiAlH4 to give (RS)-2-amino-4-phenyl-butan-1-ol (3.6 g, 78%, MS: m/e=166 (M+H+)) as a light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06184236B2 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-922d82ec72894955b59b642a49546f4e |
| Source note | uspto-grants-2001_02 |