HuagongsheHuagongshe Chemistry Print Report · For research reference only
Aluminium lithium hydride → HCID 21260549, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | HCID 21260498 | HCID 21260498 | — |
| Product | HCID 21260549 | HCID 21260549 | 17.2% |
Reaction Steps
Following the procedure of example 40b, N-[1-(4-benzyloxy-phenyl)-piperidin-4-yl]-4-phenyl-butyramide (450 mg) was reduced with LiAlH4 to give [1-(4-benzyloxy-phenyl)-piperidin-4-yl]-(4-phenyl-butyl)-amine (75 mg; 17%) as a light yellow solid (MS: m/e=415.4 (M+H+)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06184236B2 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-88c04ee563ee4a689f96c36313bfe48d |
| Source note | uspto-grants-2001_02 |