HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69145286, compound → HCID 21876989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69145286 | HCID 69145286 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21876989 | HCID 21876989 | 83.2% |
Reaction Steps
A mixture of 4-[4-(3-phenylureido)benzyl]phenyl-carbamic acid benzyl ester (1.3 g) and 10% palladium on carbon (0.35 g) in ethanol (150 mL) was hydrogenated at 50 psi in a Parr apparatus for 12 hours. The reaction mixture filtered through a Celite pad to remove catalyst. The filtrate on concentration gave 4-[4-(3-phenylureido)benzyl]-phenylamine (0.76 g) as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06184242B2 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-caf6c8bac71f4940814282c5b12b6ba9 |
| Source note | uspto-grants-2001_02 |