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4-(4-Benzylaminosulfonylmethylbenzyl)-nitrobenzene → 4-(4-Benzylaminosulfonylmethylbenzyl)-phenylamine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 4-(4-Benzylaminosulfonylmethylbenzyl)-nitrobenzene | HCID 21876751 | — |
| 触媒 | Palladium | HCID 23938 | — |
| 溶媒 | Ethyl Acetate | HCID 8857 | — |
| 生成物 | 4-(4-Benzylaminosulfonylmethylbenzyl)-phenylamine | HCID 21876959 | 95.9% |
反応手順
A solution of 4-(4-benzylaminosulfonylmethylbenzyl)-nitrobenzene (44 mg) was dissolved in ethyl acetate and hydrogenated at 40 psi with 10% palladium on carbon catalyst for 2 hours. The mixture was filtered, and the solvent was evaported to give 4-(4-benzylaminosulfonylmethylbenzyl)-phenylamine (39 mg) as an off-white solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06184242B2 |
| 出典データセット | uspto-grants-2001_02 |
| ORD ID | ord-10a620ee54fe432099073948578b0a51 |
| 出典メモ | uspto-grants-2001_02 |