HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 18335068, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86756367 | HCID 86756367 | — |
| Product | HCID 18335068 | HCID 18335068 | — |
Reaction Steps
Treatment of N-[(1-methyl-3-isobutyl-indole-2-carbonyl)cyclohexylalaninyl]-3-amino-5-(2,6-dichlorobenzoyl)oxy-4-oxo-pentanoic acid, tert-butyl ester with TFA as described in Example 80 gave the titled product (54.2 mg) as a white powder. MS C35H41Cl2N3O7, [M+H]+ =686, [M−H]−=684. TLC (CH2Cl2/MeOH, 90/10): Rf=0.30.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06184244B2 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-3b8e564aaed5430ba54bd74b73bfa599 |
| Source note | uspto-grants-2001_02 |