HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dibromobutane → HCID 18328044, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dibromobutane | HCID 8056 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 18328155 | HCID 18328155 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 18328044 | HCID 18328044 | — |
Reaction Steps
950 mg of 4,5-dihydro-3,7-dimethyl-1,4-benzoxazepin-5-one was dissolved in 30 ml of acetone, 4.3 g (4 equivalents) of 1,4-dibromobutane and 2.1 g (3 equivalents) of potassium carbonate were added, then the resultant mixture was heated and refluxed for 10 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06187769B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-5fc6ce5875a34028a9a05710f4f8fda6 |
| Source note | uspto-grants-2001_02 |