HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,5-Dibromopentane → HCID 18328111, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,5-Dibromopentane | HCID 8100 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 18328155 | HCID 18328155 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 18328111 | HCID 18328111 | — |
Reaction Steps
346 mg of 4,5-dihydro-3,7-dimethyl-1,4-benzoxazepin-5-one was dissolved in 20 ml of dimethylformamide, then 88 mg (1.2 equivalents) of 60% sodium hydride was added. This was agitated for 30 minutes, then 1.68 g (4 equivalents) of 1,5-dibromopentane was added and the resultant mixture was agitated at room temperature for 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06187769B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-97de8bf809914dbea7fcf886767c3c4c |
| Source note | uspto-grants-2001_02 |