HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9903258, compound → HCID 9859317, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9903258 | HCID 9903258 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 9859317 | HCID 9859317 | — |
Reaction Steps
A suspension of the compound of Procedure example 1 in ethyl acetate is extracted by shaking several times with a concentrated aqueous sodium bicarbonate solution; the ethyl acetate phase is then dried over sodium sulfate, filtered and concentrated in vacuo. 6-Chloro-2-methyl-8H-indeno[1,2-d]thiazole is obtained with a melting point of 94° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06187801B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-4f90fb39fbd345b7a1a31208ac476bf6 |
| Source note | uspto-grants-2001_02 |