HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Bicarbonate → HCID 22168674, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 22168559 | HCID 22168559 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 22168674 | HCID 22168674 | — |
Reaction Steps
Reduction of the above nitro compound by the method of Example 2, except that the solvent was methanol, and NaHCO3 solution was used to basify, gave allyl 2-allyloxy-5-aminobenzoate. Nmr (CDCl3): δ 3.23 (br, 2H); 4.53 (dt, 2H); 4.79 (d, 2H); 5.21-5.49 (m, 4H); 5.93-6.14 (m, 2H); 6.80 (m, 2H); 7.16 (d, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06187804B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-780327e14798400fad361b4b635027cb |
| Source note | uspto-grants-2001_02 |