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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 635391Generated: October 30, 2026

Sodium Bicarbonate → HCID 22168674, compound

https://huagongshe.com/reaction/635391

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 22168559HCID 22168559—
SolventMethanolHCID 887—
ProductHCID 22168674HCID 22168674—

Reaction Steps

Reduction of the above nitro compound by the method of Example 2, except that the solvent was methanol, and NaHCO3 solution was used to basify, gave allyl 2-allyloxy-5-aminobenzoate. Nmr (CDCl3): δ 3.23 (br, 2H); 4.53 (dt, 2H); 4.79 (d, 2H); 5.21-5.49 (m, 4H); 5.93-6.14 (m, 2H); 6.80 (m, 2H); 7.16 (d, 1H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06187804B1
Source datasetuspto-grants-2001_02
ORD IDord-780327e14798400fad361b4b635027cb
Source noteuspto-grants-2001_02