HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18615253, compound → HCID 18615157, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18615253 | HCID 18615253 | — |
| Reactant | Ethylacetate methanol | HCID 21584119 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 18615157 | HCID 18615157 | — |
Reaction Steps
According to the procedures as given in Example 2, the compound of Example 24 (in a solution of 40 mg of the compound in 5.1 ml of methanol) was subjected to a hydrogenolysis using 10% palladium/carbon black (24 mg), whereby the above-identified compound (38.3 mg) was obtained. Rf=0.38 (methanol/ethyl acetate of 1/3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06187809B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-8377adacb10e4794b2794acf17f9c648 |
| Source note | uspto-grants-2001_02 |