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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 635804Generated: October 29, 2026

Bromine → 6-Bromo-2,4-dimethyl-2,3,4,5-tetrahydro-1,2,4-triazine-3,5-dione

https://huagongshe.com/reaction/635804

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBromineHCID 24408—
Reactant2,4-Dimethyl-1,2,4-triazine-3,5-dioneHCID 313452—
SolventWaterHCID 962—
Product6-Bromo-2,4-dimethyl-2,3,4,5-tetrahydro-1,2,4-triazine-3,5-dioneHCID 260563—

Reaction Conditions

Temperature60 °C

Reaction Steps

The compound 17a (13.3 g, 94.1 mmol) is placed in 100 ml of water in the presence of bromine (18 ml, 351 mmol) and then this mixture is heated at 60° C. for 12 h.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06191130B1
Source datasetuspto-grants-2001_02
ORD IDord-2c58781151b84d50aca03a2bb431083a
Source noteuspto-grants-2001_02