HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthalenesulfonyl chloride → HCID 9824070, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthalenesulfonyl chloride | HCID 66560 | — |
| Reactant | Sodium bis(trimethylsilyl)amide | HCID 2724254 | — |
| Reactant | HCID 9837670 | HCID 9837670 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 9824070 | HCID 9824070 | — |
Reaction Steps
from 3-(octahydro-7-indolizinyl)-1-H-4-azaindole (more polar isomer) (22 mg, 0.091 mmol), 1-naphthalenesulfonyl chloride (38 mg, 0.18 mmol) and 1M NaN(TMS)2 (200 μL, 0.10 mmol) in THF (2.5 mL) at RT.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06191141B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-4ec083b873864f07b4255bde023870e0 |
| Source note | uspto-grants-2001_02 |