HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenylacetic Acid → 2-(phenylacetamido)butyric Acid Iso-butyl Ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenylacetic Acid | HCID 999 | — |
| Reactant | Isobutyl 2-aminobutyrate | HCID 13743360 | — |
| Product | 2-(phenylacetamido)butyric Acid Iso-butyl Ester | HCID 54176777 | — |
Reaction Steps
Following General Procedure H′ above and using phenylacetic acid (Aldrich) and iso-butyl 2-aminobutyrate (prepared following General Procedure J′ above), the title compound was prepared. The reaction was monitored by tlc on silica gel and purification was by chromatography on silica gel using 9:1 toluene:EtOAc as the eluant.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06191166B1 |
| Source dataset | uspto-grants-2001_02 |
| ORD ID | ord-83169bb0febf4bd8a9c4d66b6495a72b |
| Source note | uspto-grants-2001_02 |